Ku China, zinthu zambiri zamankhwala, zopangidwa zina zamankhwala, zolengedwa zolengedwa, ndi zina zotere. Chifukwa cha kuchuluka kwa zitsanzo, ambiri aChromatographic zitsanzo mabotolo Muyenera kutsukidwa pakuwona, zomwe sizimangokhala nthawi yogwira ntchito, komanso nthawi zina zimapangitsa kupatuka kwa zoyeserera kwa mabotolo a chromatographic mutatha kuyeretsa.

Kuyeretsa kwa mabotolo a chromatographic ndikofunikira kwambiri. Malinga ndi njira yotsukira ya chida chagalasi, sankhani njira yoyeretsa malinga ndi digiri ya kuwonongeka, palibe njira yokhazikika. Njira Yachidule:

Yankho 1:

1. Thirani ndikuuma madzi muchromatographic sample vial.

2. Thirani zowuma zitatha izi pamene mowa umalowa mu 1.5ml vial mosavuta ndipo amasungunuka ndi ma solfordic ambiri

3. Thirani m'madzi ndikusamba ndi akupanga kawiri.

4. Thirani madzi mu botolo ndikuphika pa 110 ° C kwa maola 1 ~ 2. Osaphika kutentha kwakukulu.
5. Zabwino komanso kusunga

Scheme 2:

1. Adzatsuka madzi opondera kangapo

2. Ikani mu beani yodzaza ndi madzi oyera ndi ultrasound kwa mphindi 15

3. Sinthani madzi ndi ultrasound kwa mphindi 15

4. Zilowerere mu chomera kapena chopanda ethanol

5. Tenga Zui ndi Kuuma

Mukufuna kudziwa momwe angasinthire vials yosiyanasiyana ya HPLC ?, Onani nkhaniyi:CR. CRAIL VS. SNAP VS. Screct Cap Vial, momwe mungasankhire?

Yankho 3:

1. Zilowerero ndi methanol (chromatographic yoyera) ndi yoyera ndi akupanga kwa mphindi 20, kenako kutsanulira methanol youma

2. Dzazani botolo lachigawo ndi madzi, nadzatsuka ndi akupanga kwa mphindi 20, ndikukhetsa madzi

3. Pambuyo poumaMbale ya HPLC

Yankho 4:

1. Nthawi zambiri amagwiritsa ntchito madzi oyera amawuma kenako ndikugwiritsa ntchito sulfate dziratani potaziyamu wotchera

2. Njira yotsuka ya chromatographic yachitsanzo yofanana ndi gawo lamadzi. Choyamba, kumwa mankhwala azachipatala kumachitika kuti zilowerere kwa maola opitilira 4, kenako akupanga kwa theka la ola

Yankho 5:

1. Ngati mtengo wake ndi wokwanira, gwiritsani ntchito zui yatsopano nthawi iliyonse

2. Ngati mukufuna kugwiritsidwanso ntchito, njira yotsuka ndiyofunikanso, choyamba ndi njira yoyeretsera ya oxidation

3. Mabotolo abotolo ayenera kusinthidwa ndi atsopano, makamaka popenda zotsalira za mankhwala ophera tizilombo, apo ayi zochulukirapo zidzakhudzidwa

Mukudziwa zambiri za momwe angayeretsere ma chromatography y, chonde onani nkhaniyi:Zothandiza! Njira 5 zoyeretsa ma chromatography

Zomwe zili pamwambazi ndi njira zisanu zoyeretsa zamabotolo zitsanzo za chromatographic, tikuyembekeza kuti titha kuyang'ana kutsukidwa kwa mbale za HPLC.

M'mbuyomu:

ChroMophiphy imagwiritsa ntchito Mbale Zopanda Nyuzi ndi HPLC Syngenge

Ena:

Momwe mungavale 20ml ya chromatograph vial

Ma tag: HPLC-Autosampler-Valis 2ml-gc-vial 2ml-zitsanzo-zamtengo vial-1.5ml

Kufunsa