Musoro Gasi Chromatography Sampule Kugadzirira
Kugadzirira kwemuenzaniso kwakakodzera kunokosha kuti uwane ruzivo rwakakwana uye rwunoita mumusoro musikeprishing chromatography kuongorora. Matanho anotevera ataure nezve kufunga kwekutanga kwekugadzirira samasemu emusoro kuongororwa kwemusoro.
1. Sarudza iyo chaiyo samplu vial
Kusarudza iyo chaiyo samplu vial kwakakosha kuti ubudirire mumusoro sampling. Saizi dzakajairika dzinosanganisira 6ml, 10ml, ne20ml, ine 20ml vials ichinyanya kushandiswa. Zvinhu zvakakosha kufunga kana uchisarudza vials zvinosanganisira:
Zvinyorwa: vials zvinowanzogadzirwa negirazi kana mapurasitiki. Magirazi magirazi ari nani kuremerwa kwemasampuli emisiki nekuda kwekuita kwavo uye mukana wekusvibisa kusvibiswa kusvibiswa.
Sungai macaling mechanism: vials inogona kuisirwa chisimbiso pamwe nekapepa kana screw kapu. Varume vepamusoro vanopa chisimbiso chemagetsi, icho chakanyanya kukosha kuchengetedza kutendeka kwemusoro.
SEptum quality: Secsa inoshandiswa kusimbisa vials inogona kuunza zvinomutsa kana ivo vari vane kunaka. Tarisa seSista yakagadzirirwa zvakananga kumumusoro mashandisirwo, sezvo ivo vasingakwanisi kusevha mumusoro.
2. Muenzaniso Vhoriyamu uye Dufiution
Iro vhoriyamu yemuenzaniso mune vial inokoshesa kuwana iyo yakakwana yemusoro wekusangana. Kazhinji, iyo sampula vhoriyamu inofanira kunge yakatenderedza 1 \ /3 kusvika 1 \ / 2 yehuwandu hwakazara hwesual kuti upe mupendero wakakwana wechikamu chegesi.
DILUILUtion: Kana kushamwaridzana kwakanyanya, kunogona kuguma nemusoro wakazadzwa, zvichitungamira kuccurate. Kutsiva sampuli ine yakakodzera solvent inogona kubatsira kuzadzisa iyo yaunoda kusunganidzwa kwekuongororwa kwechokwadi.
3. Tembiricha kudzora
Tembiricha inoita basa rakaoma muMusoro Sampling sezvazvinoshamwaridzana nezvokuenderana neyekuongororwa uye kupatsanurwa kwavo muchikamu chegesi.
Kupisa kuenzanisa: Mirimo yemuenzaniso inofanira kuiswa kune inodziya tembiricha kusimudzira kusunungurwa kwemavheni mumusoro. Iyo tembiricha yakakwana inotsamira pane chaiyo yekuongorora kuongororwa uye inofanira kutsanangurwa panguva yekuvandudza nzira.
Nguva yekuenzana: Bvumira nguva yakakwana yemuenzaniso kuti usvike kuenzana. Izvi zvinogona kusiyanisa zvichienderana nesemuenzaniso matrix uye kuderera kwemakomputa. Chaizvoizvo kuenzana kuenzana kubva pamaminitsi makumi matatu kusvika maawa akati wandei.
4. Regedza kusvibiswa
Kusvibiswa kunogona kukanganisa zvakanyanya kujekesa kwemusoro kwegirasi gasi chromatography. Kuti uderedze njodzi yekusvibiswa, ita zvinotevera:
Shandisa pre-yakacheneswa vakunda
Nzira YEMAHARA: Mhanya nzira dzakabikwa kuti dzione zvinowanikwa zvekusvibiswa. Izvi zvinosanganisira kuongorora sampuro isina chinhu uchishandisa kugadzirira kumwechete uye maitiro ekuongorora kuti uone kuti hapana mapenzi asina kudiwa achizoonekwa muChromatorm.
Mamiriro ekunze akatodzidzira: Ita kugadzirira kwemuenzaniso munzvimbo yakachena yekudzora kuratidzwa kune mhepo inosvibiswa.
5. Sarudza iyo chaiyo misoro nzira
Sezvambotaurwa, mumusoro sampling inogona kunge iri yemitambo kana ine simba. Iko kusarudzwa kwehunyanzvi kunoenderana nekunyorera chaiko uye chimiro chemuenzaniso.
Static Musoro: Iyi nzira yakakodzera kune akawanda mashandisirwo uye anoshandiswa zvakanyanya kuongorora mishonga inoshamisa mune zvinwiwa uye solids. Izvo zvinobvumira ongororo kune zvakasikwa kupatsanurana mumusoro pasina iyo yekutanga kwegadziriro yekuwedzera.
Dynamic Musoro: Iyi nzira iri nani yakakodzera samples dzinoda kuchenesa kuenderera mberi kuti utore mishonga inosimbisa. Izvo zvinowanzoshandiswa mukushandisa zvakadai sekuongororwa kwezvakatipoteredzwa uye kuongororwa kwechikafu uko samples inogona kuve neyakaderera fungidziro yekuongorora.
