Samfurin vial yana da babban tasiri. Yana shafar tsari da sakamakon cututtukan cututtukan cututtuka. Idan samfurin vial ya tsabtace ba daidai ba, zai gurbata shi. Wannan gurbataccen na iya haifar da: lalata ƙwayar cuta, lalacewar samfurin, wanda aka bincika asara, maimaitawa da ƙarfi, da kuma kololuwa maimaitawa da sauran ƙarfi kuma septum ma'amala. Da kyau m manace vials zai iya shafan sakamakon gwajin. Wannan zai haifar da karkacewa a cikin sakamakon har ma lalata autosampler.

Saboda haka, tsaftacewaAutosampler vialyana da matukar muhimmanci. Mai binciken dole ne ya mallaki hanyar tsabtace ta Vial.

Kuna son sanin cikakken bayani game da HPLC Vials, don Allah a duba wannan labarin: Encyclopedia na HPLC VIals

Yadda ake

Hanyar wankin ya bambanta bisa ga matsayin gurbataccen vial. Wannan talifin zai bayar da shawarar hanyoyi da yawa don tsabtace Vial. Za su taimaka muku gama gwajin Chromatographic.

Hanyar 1

1. Zuba maganin gwajin a cikiHPLC Vial.

2. Nutsad da duka vial a cikin 95% barasa a cikin 95% mai tsabta shi sau biyu, sannan kuma zuba shi bushe (babban taro na barasa ya shiga ciki tare da yawancin abubuwan sha na kwayoyin halitta).

3. Zuba cikin ruwa mai tsabta da kuma ultrasonically tsaftace shi sau biyu.

5. Sannu da kantin sayar da kaya.

Hanyar 2

1.rinse sau da yawa tare da famfo famfo.

2. Rarraba shi a cikin mai ɗorolder na ruwa mai narkewa da amfani da daskararren tsabtace na ultrasonic har minti goma sha biyar.

3. Byauki ruwa kuma ka ba shi wani mintina biyar na tsabtace na ultrasonic.

4. Rushe vial a cikin ethydrous ethanol-cike mai saiti.

5. A karshen, cire shi kuma a bar shi ya bushe a zahiri ta bushe.

Hanyar 3

1. Jiƙa shi a cikin methanol na mintina ashirin, sannan cire methanol kuma tsaftace shi tare da ultrasonography.

2. Bayan daɗa ƙarin ruwa zuwa ga samfurin vial, Ultrasonic mai tsabta yana tsaftace shi na minti 20, sannan magudana ruwan.

3. Bada izininviala bushe.

Hanyar 4

1. Kura kuma bushe shi da tsabtataccen ruwa da farko, sannan jiƙa shi a cikin mai karfin iskar shaye shaye shaye masu tsabta (potassium dichrozate) tsabtatawa.

2. Jiƙa a cikin barasa barasa na sama da sa'o'i 4, to, tsabta barasa na rabin sa'a don rabin sa'a, kurkura da ruwa da bushe.

Hanyar 5

1. Jiƙa a cikin karfin tsabtatawa na tsabtatawa na tsawon awanni 24.

2. Tsabtace sau 3 tare da narkewar ruwa a karkashin yanayin ultrasonic, kuma a ƙarshe tsabtace sau ɗaya tare da methanol, kuma bushe shi don amfani.

Hanyar 6

Yi amfani da wanke iska. Mashin wankewar kwalban na iya inganta ingancin tsabtace vials da kuma adana mutum da lokaci.

Shin kun san ƙarin yadda ake tsaftace vials ɗinku na HPLC? Duba wannan labarin: Hanyoyin tsabtatawa guda biyar don HPLC VIals

Matsalolin da zaku gamu da juna

Akwai matsaloli da yawa tare da tsabtatawa mai tsabta.

1. Karancin tsabtatawa, lokacin wanka mai dogon lokaci, cinya lokaci da ƙoƙari. Bugu da kari, yawan goge da kayan wanka suna da girma, suna da wahalar sarrafawa, kuma bata albarkatun ruwa.

2. Tsabta yana da yiwuwa ga matattu sasanninta, tsaftace sakamako yana da wuya a tabbatar da cewa yana haifar da sakamakon gwajin, kuma yana ƙaruwa da ikon da kayayyaki.

3. Akwai haɗarin aminci a cikin tsabtatawa na ma'aikatan tsabtace ma'aikata. Wasu dalilai za su yi amfani da injunan tsabtace na ultrasonic. Wannan hanyar tsabtacewa tana inganta ingancin tsabtace da tsabta zuwa wani gwargwado, amma kuma yana da rashin amfanin gona.

Injin tsabtace ultrasonic shine mai amo da matsananci yayin aikin aiki, kuma yana da sauki karya vial, kuma lokacin tsabtatawa ba shi da sauki a fahimta. Sabili da haka, muna ba da shawarar cewa kuna sa safofin hannu, goggles, kunnen kunne da sauran kayan aikin kariya na kariya yayin tsabtatawa.

Idan vial ya tsufa ko lalacewa, kada ku sake amfani dashi. Ya danganta da sau nawa kuke yin gwajin, maye gurbinsamfurin vialkowane watanni 1-3.

Yankakken vials suna buƙatar sarrafawa a gaba ɗaya, an kula da shi daidai da ka'idojin gudanarwar kayan shakatawa na lalata, kuma ya kai ga cancantar lalata jiyya na lalata.

Kowane hanyar tsaftacewa tana da amfani da rashin amfani. Hanyar mafi kyau ita ce maye gurbin sabon vial bayan kowace gwajin. Yana da mahimmanci ku zaɓi dabarar tsabtatawa ta dama. Dangane da nau'in samfurin gwaji da yanayin dakin gwaje-gwaje na ainihi, wannan zaɓi ya kamata a yi. Yana kuma da kyau a lura da lamarin shari'ar. Ya kamata a tuna cewa bin kowane gwajin chromatographic, septum na samfurin vial yana buƙatar maye gurbinsa.

Wan don sanin cikakken ilimi game da yadda za a tsabtace samfurin Chromatography ba, don Allah bincika wannan labarin: Ingantacce! 5 Hanyoyi don tsaftace kayan chromatographography

A baya:

Select da ingantaccen HPLC vials don inganta binciken HPLC

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