Nā Vials haʻahaʻa haʻahaʻa haʻahaʻa, Vial

Ma nā loiloi kiʻekiʻe-kiʻekiʻe,ʻo ka poho adsorption e hiki ai i nā papa hana he palena hiki ke kaupalena i ka pololei. Nā pūʻulu Silanol Rilanol ʻO nā Vialilicate kūpono e hāʻawi pinepine i nā lāʻau lapaʻau polar a iʻole bioomolecule i lalo o ka 80%, a me nā hale kūʻaiʻo Automated Manaʻo nā Vendors i nā aniani aniani silaanimized no ka hoʻopiliʻana i nā popo nui i ke aniani No laila, he koʻikoʻi a iʻole keʻano o ka papaʻana no ka pae kiʻekiʻe.

2. Nā wahi aniani o nā aniani a me nā mea hana adsorption

A. Nā hui Silanol a me nā mea hao
  i. Nā papa hanaʻo Si-Oh Get Bind Bind Play Plar
  II. Trace Metal ions hana koho balota Electrostatic pili me nā Molecules

b. Shop
  i. ʻO nā mea hana kūlohelohe (E.G., ACN, Meoh

c hoowela. Halihali iho
  i. ʻO nā mea i hoʻopiʻiʻia a iʻole hydropphilic paha nā molekula ma ka paia e hana i nā peak ghots spies ma hope

d. Nā hopena'ōnaehana automated
  i. Nā mea i hoʻopili pinepineʻia i nā'ōnaehana kikowaena kiʻekiʻe e hoʻonui ai i ka polaha a iʻole nā ​​loiloi trace
  II. Ua hōʻike pinepineʻia ka nalowale hōʻailona ma mua o 10% i ka manawa

3

3.1 Ke kūleʻa kūloko

A. ʻO keʻano kiʻekiʻe-kiʻekiʻe (~ 800 ° C)
  i. E holoi i kekahi mau sii-oh

b. Holoi holoi (e.g., 6 m hcl)
  i. Hoʻopau i nā Iakai Metala akāʻo Roughens

c hoowela. Wale Wa holoi (E.G., 1 M Naoh)
  i. Hana i nā pūnaewele si-O-ONT, counterctive

d. PAHUI
  i. ʻO ka hapaʻokoʻa wale nō o nā pūnaewele ikaika ma ke aniani

3.2 Silaanization

A. ʻO Orngeosalane ma lalo o ka hakahaka
  i. ʻO Janisolisilanes (e.g.,ʻo MitylsLilane) hana i nā hui SI-O-si i nā cilanols
  II. Hana i kahi pale hydrophobic e puka ana i ka wela wela, acids, a me nā waihona
  III. ʻO ka haʻahaʻa haʻahaʻa haʻahaʻa a hoʻihoʻi hou i ka hoʻonuiʻana i ka polar e hoʻihoʻi hou i luna o 90%

b. Nā hiʻohiʻona Vendor
  i. "DV" Silaanized Vials no ka helu helu Polar-Compoundis (wai)

3.3 mau'ōpiopio hana

A. Perfluorodecdectlrosilrosilsilla (pfdcs)
  i. Ua hōʻuluʻuluʻiaʻo ia iho i ka monolayer e hāʻawi ana i ka papa superhydrophobophobophobophobop
  II. Kūpono no nā poʻe nonpolar Pahs a me Lipid-sollable

b. PolyTeTyyne Glycol (peg)
  i. ʻO nā pūpūʻo Hydrophilic Prendin i hana i nā protein
  II. Hāʻawi i ka palekana o ka bioomolecules

4.ʻO ka hoʻopiliʻana o ka hoʻolahaʻana o ACTSORCT

A. Nā hopena hoʻolaha
  i. ʻO Silane mau mea e hoʻihoʻi i ka hydrophobic hydrophobic, paleʻole i ka popo polar
  II. Paʻa ma hope o ka hoʻonuiʻana i ka maʻi nui ma ACN a iʻole Meoh

b. Hana Hou
  i. Mālamaʻo Silanized Vialized ma kahi kokoke-100% no ka 1 ppb dexepin ma luna o ka manawa
  II. Loaʻa i nā VIAT-COIAT VIAS i loaʻa 97-99% e hoʻihoʻi no ka polar β-lactamts ma luna o 72 hvers 70-80% ma kahi aniani
  III. PFDCS Vials ma mua o 90% hoʻihoʻi no nā pahs i hoʻohālikelikeʻia i nā waiwai haʻahaʻa haʻahaʻa

c hoowela. ʻO ka hoʻonohonohoʻana i ka hoʻolahaʻana
  i. Nā Helu POPLA: Peg> silananiini ≈ pfdcs> diCattivated
  II. Nonplar

5.ʻO ke koho noi a me nā hana maikaʻi loa

A. E hoʻohālikelike i ka hoʻomaʻamaʻaʻana i ka Chemple Chemple
  i. ʻO nā mea hoʻohui Polar
  II. ʻO nā Onches Onches (Pahs
  III. Nā helu i huiʻia: Hāʻawiʻo Silananization i ka hana kaulike

b. E noʻonoʻo i ka hoʻokele a me ka nohona
  i. Silane Coatings Tolerate PH 1-12 a me nā mea hana maikaʻi loa
  II. Hiki i nā lole polymer ke hoʻonuiʻia ma lalo o nā oridizers ikaika a iʻole ka wela kiʻekiʻe; E noʻonoʻo i nā mea i hoʻopaʻaʻia paha PTFE a iʻole PypPylene Vialits no nā kūlana koʻikoʻi

c hoowela. Sample volume a me ka hopena injection pinepine
  i. No nā microvolus
  II. Monitor Coating Integrity ma o ka hoʻopiliʻana i ka Angle (> ± 10 ° °

d. Kālā kālā
  i. DACCTIVIVATION:ʻO ke kumukūʻai haʻahaʻa, kūpono no ke aʻoʻana a iʻole nā ​​papa hana maʻamau
  II. Silanized Vial
  III. Peg \ / pfdcs coatist: kumukūʻai kumukūʻai, kūpono no nā biona koʻikoʻi

6.ʻO ka hopena: mai ka Hale Kūʻai Kūʻai i nā interface ikaika

E like me kaʻikeʻana o kaʻikeʻana i ka ppb \ / ppc pae, e lilo i nā hua'ōlelo likeʻole ma mua o nā mea kūʻai passive. Ua kohoʻia nā hana haʻahaʻa haʻahaʻa haʻahaʻa haʻahaʻa e hoʻohuli i nā pohoʻole i nā pohoʻole i loko o nā'āpana paʻa. ʻO ke koho Vial a me ka mālamaʻana i ka mālamaʻana i nā mea nui i nā mea nui ma ka haʻahaʻa haʻahaʻa haʻahaʻa. Ma ka hoʻokūkūʻana iʻenehanaʻenehana e hoʻohālike i ka Chemport, e hoʻohuli i nā Valsises i nā pono hana i hala a me ka hana houʻana i ka hana kuhihewa.

Nā hana nui

1. No nā loiloi Ultra-sensitive, hoʻohana i nā vial i hoʻopaʻaʻia a iʻoleʻia

2. E hoʻohālikelike i nā polarity: Silanized \ / Peg no ka hydropphilic, pfdcs no ka hydrophobic

3. Monitor Coating: E ​​mālama i nā papa hoʻomaʻemaʻe, Track i nā kihi, e holo i nā papa, e hoʻololi i nā pale, hoʻololi i ka hāʻuleʻole

4. ʻO ke kaulike kumukūʻai vs.ʻO ka maikaʻi o kaʻikepili: nā lole kūʻai Premium e hōʻemi ana i nā reruns a me nā mea maʻamau