Site na mmiri acidic na ọgwụ ọjọọ, na-ahọrọ oke nlele anya na-ezighi ezi nwere ike ị nwetaghachi ma ọ bụ na-akpalite phantom phantom. Ntụziaka a na-akpata oke nke soda-wayo vs. borogicilate iko ma na-enye usoro vil-na-sera na-eme nchọpụta na-eme nyocha - iweghachi nrụpụta sitere na nchịkọta ihe.

Ihe nlele gị na ntinye akwụkwọ

Ndostri	Nlele anya	Mkpa akpa dị mkpa
Gburugburu ebe obibi	Acidic Isthewoter (ph 1-3)	Iguzogide iguzogide iguzogide; Eut Metal Liach
Plama r & d	Apis etisawo na acetonitrael	Nguzogide uzo; Mgbasa ozi dị ala
Nnwale nri	Rọrọ na mmanụ oriri	Ndakọrịta lipophilic; Nchedo ọkụ

Ntụnyere arụmọrụ arụmọrụ

Mgwooru	Akparamaagwa	Mmetụta kemịkalụ	Akwụ ụgwọ (€ kwa vial)	Jiri ikpe
Iko lime	Ọ dịkarịa ala ọnụ	ph 6-8 naanị	~0.5	Achinglọ Labks; mmiri dị mkpụmkpụ
Obere-boalilicate	Na-eguzogide acid acid (ph ≥4)	Ọ bụghị hf- ma ọ bụ nnukwu na-eguzogidesi ike	★★☆☆☆	Mmiri Hplc
Na-agbaze mmiri	ph 0,5-10; Autoclaveble na 120 Celsius C	Pọm sh; okpomọkụ	★★★☆☆	Phirama QC; Ihe nlele
Elu-borosilicate	Ph 0-14; na-akwụsi ike	Niile acid \ / ntọala; 500 Celsius C	★★★★☆	Chọpụta \ / Acid-acid

Mara: Ọgwụ-borosilicate na-ezute USP \ /P na-enweghị ọgwụ. Bobosolicate CTTE ≈3.3 × 10⁻⁶ \ / k na 9 × 10⁻⁶ \ / k maka iko nkịtị.

Na-ahọpụta Septeka ziri ezi

Seldị nkebi	Ndụ Ndụ	Mmetụta kemịkalụ	Ngbata	Ezigbo maka
PTFE \ / silicone mejupụtara	15-20	Acid, ntọala, sochiri anya	DMF nwere ike ihichapụ	HPLC Autosampler na-agba ọsọ
PTFE	Otu eji	Ihe Mgbakwunye Niile Organic	Akara mmachi	GC-MS HAYENAD
Pre-saracone	30+ Dedcings	Acid \ \ / ASES (PH 3-10)	Na-ekwu na acetone	Nseta ihuenyo dị elu

Nkwado Vial & Prepo site na nlele

Ụdị atụ	Na-atụ aro vial	Nnukwu nhọrọ	Ọnyà ga-ezere
Industriallọ Ọrụ Instaial (PH 1.5)	Vial-borosilicate doro anya	White Ptfe \ / silicone mejupụtara	Ejila soda-wayo (gbazee na 24 h)
Ọgwụ ọjọọ na acetonitrael	Vial-borialolicate vial	Blue PTFE	Na-eduga na-eduga na-eduga na ọdụ ụgbọ elu
Mmanụ mmanụ oriri	Amber elu-borosilicate	Pre-saracone	Iko doro anya chọrọ nchebe ọkụ
Na-akuzi buff (anọpụ iche)	Soda-lime iko	Ọkọlọtọ Silcone	Naanị maka obere oge, ebe nchekwa

Ọmụmụ okwu: Ntinye usoro mbufe na Plampma

Mbido mbido:
- Sọle: API na 0.1% acid \ / acetonitrile (1: 1)
- Akpa: VIALS-Borosilicate VICENCOON Sepum
Isi Okwu:
- A na-amabeghị ọnụ ọgụgụ ndị a na-amaghị ama na-apụtaghị na ntụtụ # 3 (silicone ndị na-agba akwụkwọ)
- API ọdịnaya dara na 12% mgbe elekere 72 H (Adsgba Admiorption)
Ngwọta:
- Kwalite na-egbutu ihe na-egbu egbu
- Tụgharịa gaa na PTFE \ / silicone mejupụtara conta (Pre-POONDED 5 ×)
Nsonaazụ:
- Phantom Phantors wepụrụ
- Nnwale ule dị iche iche <0.8%

Ihu na-aga

Harsh acid → Oke-borosilicate
Mgbapụta Pharlọ Ọrụ Phita Arma Mkpesa-borosilicate
Atụmatụ nlele nke na-adịghị ike → soda-wayo-wayo
PAMA Chemistry> Mmanyapu ndu

Nkọwa data:

USP <660> eji akpa iko
Akụkọ nyocha nke CACEDICED

Site na ntuziaka a, kwekọrọ na VIL na Sepum lyruction - zere ngwa ahịa dị ọnụ ma hụ na ọ ga-arụpụta ihe na nyocha nke ụlọ na ọgwụ.

Nke gara aga:

Kedu ihe dị iche na GC-MS na GC-MS \ / MS?

Osote:

Laghachi na ndepụta

Tags: Hplc vials GC-MS Sample prep vials na-agba iko dị elu vials-boalili mkpa iko PTFE \ / silicone capra

Njuputa