Mai le malosi o le vai o le acidic i lipophilic fualaau faasaina, filifili le sese o le tele o faʻataʻitaʻiga e mafai ona toe maua le toe faʻaleleia o le phantom. O lenei taiala na te faʻaalia le faʻatinoina o le sooga o le soda-lie vs. borosisicate tioata ma ofoina atu ni fetuunaiga-ma-septa o loʻo foia ai le faʻaaogaina o mea sese.

Lau faʻataʻitaʻiga & talosaga manaʻoga

Alamanuia	Faataitaiga masani	O le mea autu e manaʻomia
Siosiomaga	Acidic otaota (ph 1-3)	Afaina ai le afaina; zero uʻamea faʻamau
Pharma r & d	O le APIS sa soloia i Acetoniterrio	O le faʻatulafonoina o vailaʻau-faʻaola-faʻaola; maualalo adderption
Faiga taumafa	Palasitika i totonu o suauu suauu	LUPOPPILILIC i le fetaui; Malamalama moli

Mea Faatino Aiaiga

Meafaitino	O uiga taua	Taaloga talafeagai	Tau (€ i le Vial)	Faaaoga Mataupu
Soda-lie tioata	Sili ona taugata	pH 6-8 na o	~0.5	Aoaoga labs; Vai puʻupuʻu vai
Maualalo-boronicite	ACIC ACID tetee (ph ≥4)	E le o le HF- poʻo le malosi faʻavae-tetee	★★☆☆☆	O mea masani o le HPLC Water na te totogiina
Feololo-Boronicite	pH 0.5-10; Autoclavable i le 120 ° C	Lautele ph; vevela-steriliable	★★★☆☆	Pharma qc; bio faʻataʻitaʻiga
Maualuga-boronicite	Matua o le SH 0-14; Maliu Mafutaga	Uma acids \ / poloka; 500 ° e mafai	★★★★☆	Trace \ / harsh-acid auiliiliga

FAAMATALAGA: O Medium-Borosisicate Feiloai USP \ /p psymacutical tioata tulaga faatonuina. Maualuga-borosicicate cte ≈3 × 10 \ / k vs. 9 × 10 × \ / k mo ipu masani.

Filifilia o le taumatau Septa

Septum ituaiga	Olaga Tumi	Taaloga talafeagai	Pepelo	Lelei mo
PTFF \ / sonicone tuufaatasi	15-20 Pierctions	Acids, faavae, feololo fofo	DMF e mafai suia	HPLC Autosaapicr tamoe
Mama ptfe	Faaaoga e tasi	Uma ortic fofo	Le lelei faamaufaailoga	Gc-ms halognding plaiuys
Muai-sikoa solkone	30+ tui	Vaivaiga vaivai \ / bases (pH 3-10)	Fula i le acetone	Maualuga-enstant screens

Vial & Septa Fautuaga e ala i Faʻataʻitaʻiga

Faʻataʻitaʻiga ituaiga	Fautuaina Vial	Septum filifiliga	E aloese ai mai
Alamanuia otaota otaota (PH 1.5)	Maualuga-borosisicate manino viia	Paʻepaʻe PTFE \ / Sinicone tutoʻatasi	Aua le faʻaaogaina le soda-lie (faʻateʻa i le 24 h)
Fualaau faasaina i Acetoniterriale	Feololo-Borosisicate Vial	Lanumoana mama ptfe	Maualalo-boronisicate taitai atu i le tumutumu
Fualaʻau suauʻu	Amber maualuga-boronicite	Muai-sikoa solkone	O le tioata manino e manaʻomia ai le puipuiga moli
Aoaoina Buffers (Le faaituau)	Soda-lie tioata tioata	Tulaga tutusa	Na o le taimi puʻupuʻu, o faʻataʻitaʻiga e le masani ai

Tulaga suesuega: Metotia Faʻaliliu le faʻaletonu i le Pharma

Uluai seti:
- Faʻataʻitaʻiga: API i le 0.1% o le aciccic Acad \ / Aceminiterrior (1: 1)
- Container: maualalo-borosiicite viria + tulaga sili ona lelei aptum
Mataupu:
- O tumutumu e le iloa o loʻo aliali mai i le tui # 3 (sili-sicone
- API mataupu na pa'ū i le 12% pe a uma le 72 H (Glass Adssorption)
Vaifofo:
- Faʻaleleia i le feololo-boronicite hydrolytic tioata tioata
- Alu i le mafiafia PTFE \ / Silcone Commosite Septa (muamua tuia 5 ×)
Manatu:
- O le Phantom Tapping Aveesea
- O le ORDABED SOAD DRIVERS <0.8%

Autu Auta

Harsh Actids → maualuga-boronicite
Pharma tausisia → feololo-boronicite
O faʻataʻitaʻiga o taimi puʻupuʻu
Septa Chemistry> Pierring soifua

Faamatalaga o faamatalaga:

USP <660> tioata pusa
CMA-tusi faamaonia auiliiliga lisi lipoti

Faatasi ai ma lenei taʻiala, faʻafetaui lau telefoni ma septum i le chemistry-'alo ese mai le tele o galuega ma ia mautinoa o taunuʻuga i luga o le siosiomaga ma le vailaʻau.

Talu ai:

O le a le eseesega i le va gc-ms ma gc-ms \ / m?

Le isi:

Toe foi i le lisi

Faailoga: HPLC Vials Gc-ms faʻataʻitaʻiga pre maualuga-boronisicate tioata tioata Medium-Borosisicate Glass Gress Vials Ptfe \ / silika septa

Fesili