Maitiro ekugadzirisa matambudziko akajairika ne 2ML autosamppler vials

Autosamupler valsIzvo zvinhu zvakakomba muongororo muongorori, kunyanya mukuwedzera kwekuita kwemvura chromatography (HPLC) uye gasi chromatography (GC). 2ml autosamuplerr veigial ndeimwe yemhando dzinowanzo shandiswa saizi, asi nyaya dzakasiyana siyana dzinogona kumuka panguva yekushandisa kwavo. Gwara iri rinopa kuongororwa kwakazara kwenhau dzakajairika dzakabatana ne 2ML autosamupler vals uye inopa kugadzirisa maitiro ekugadzirisa kuve nechokwadi chekunyepedzera kuita.

Chimiro che 2ML autosamupler vals

Usati waumbwa mukutsamwa mukunetsa, zvakakosha kuti unzwisise chimiro chakakosha uye basa re 2ML autosamppler vials. Aya mavuru anowanzo kusanganisira:

Zvinyorwa: Mazhinji akagadzirwa nehurombo rebhandi, iyo inodzivirira nemakemikari uye inoderedza kudyidzana nemuenzaniso.

Chimiro cheCap: Sarudzo dzinosanganisira screw kapu, Crimp caps, uye snap caps, imwe neimwe inopa macalising akasiyana ekurwirwa.

Septa: Chinhu chinonzwisisika chinobvumira sindano penje paunenge uchichengeta chisimbiso kudzivirira kubuda kwemvura kana kusvibiswa.

Wana kuziva ruzivo rwakazara nezve nzira yekuchenesa iyo chromatography sampulies, ndapota tarisa chinyorwa ichi: Inoshanda! 5 nzira dzekuchenesa chromatography sampuli

Matambudziko akajairika uye matambudziko ekugadzirisa matambudziko

1. Kuwedzeredza kweVials

Dambudziko: Kuwedzeredza kunoitika kana huwandu hwemvura mune vial inodarika kugona kwayo kunowanikwa. Izvi zvinokonzeresa kusakwana kwemusoro weiyo autosampler sindano kuti ishande nemazvo.

Zviratidzo: Zvinonzwisisika semuenzaniso jekiseni, yakawedzera cartover, kana yakakuvadzwa tsono.

Mhinduro: Ita shuwa kuti vial izere kune yakakurudzirwa mwero, kazhinji inenge 1.5ml ye2ml vial. Izvi zvinopa humusoro hwakaringana hwekusaiswa uye kuiswa kwemuenzaniso.

2. Sampula Kusvibiswa

Dambudziko: Kusvibiswa kunogona kuitika kubva kune zvisina kukodzera kubata, subandardard vials, kana kusakwana kusingaenzaniswi.

Zviratidzo: Peaks zvisingatarisirwi muChromatogram kana kushandura manhamba.

Mhinduro: Shandisayakakwirira-mhando vials uye capsyakagadzirirwa yako chaiyo application. Gara uchibata vials nemagurovhosi uye kudzivirira kubata nzvimbo dzemukati. Funga nezvekushandisa pre-yakanatswa kana yakasimbiswa vials kuti ideredze njodzi yekusvibiswa.

3. Peaks isingatarisirwi muChromatograms

Dambudziko: Mapepa asingatarisirwi anogona kuratidza kusvibiswa kana kutakura kubva pamasampula apfuura.

Kugadzirisa matambudziko:

Chenesa autosamupler zvikamu nguva zhinji: ita chirongwa chezuva nezuva chekuchenesa chezvinodhiriso chehunhu, kusanganisira syringes uye sindano.

Shandisa yakaderera yakasara vhoriyamu vials: Sarudza yakanyanya kupora vials yakagadzirirwa kuderedza vhoriyamu yakasara uye nekudzikisa njodzi yeCrossover.

4. Tsvaga block

Dambudziko: Blathage inogona kuitika nekuda kwezvinhu zvehukadzi

Zviratidzo: Hapana sampuli yakaiswa kana iyo jekiseni vhoriyamu iri kukanganisa.

Solution: Firisa sampula uchishandisa pepa rakakodzera refaira kana membrane kuti ubvise zvikamu zvitariso usati waisa mumugwagwa. Kana blackji ikaitika, suka tsono zvichienderana nemirairo yemugadziri uye funga kushandisa sindano yakakura yeViscous samples.

5. Vial kuputsa

Dambudziko:Girazi kuburikidzalsinogona kupwanya kana yakaiswa pasi pekumanikidzwa zvakanyanya, kuvhunduka kwekunyanyisa, kana kukanganisa.

Zviratidzo: Kukuvadza kwemuviri kunoonekwa pakuongorora; Muenzaniso unogona kurasika.

Solution: Bata vial nehungwaru uye dzivisa kuchinja kamwe kamwe kwekushisa. Shandisa chifukidziro chekudzivirira kana zvichidikanwa panguva yekufambisa kana kuchengetedza.

6. Varombo vane rusununguko kuvimbika

Dambudziko: Zvisungo zvisina kukwana zvinogona kutungamira mukuvapura kwezvinhu zvemhando yepamusoro kana kusvibiswa kubva kune zvekunze zvinyorwa.

Zviratidzo: Shanduko mukuongorora kusungwa nekufamba kwenguva; kurasikirwa kwemakombi akaomeswa.

Solution: Ita shuwa caps inoenderana nerudzi rwemhando uye dzakasimbiswa mushe. Kana kubata kusimbisa masampulies, funga nezvekushandisa crimp caps yekusagadzikana kwesingaperi kwechokwadi.

Unoda kuziva nzira yekusarudza iyo chaiyo cap ye chromatography yako vial, ndapota tarisa chinyorwa ichi: Maitiro ekusarudza iyo yakakodzera cap ye chromatography yako vials?

7. Kusapindirana ne autoshampleers

Dambudziko: Haasi ese mapoka anowirirana nemhando yega yega autosampler, iyo inogona kukonzera manhamba panguva yekushanda.

Zviratidzo: Kwakashata kweVials kana kusakwanisa kumisikidza samples.

Solution: Simbisa kuwirirana kwemhando yeVial ine autosampler modhi usati washandiswa. Tarisa uone kufambisa gwara rekurudziro yakakurudzirwa.

8. Tembiricha dzinotonhora

Dambudziko: Kupisa shanduko panguva yekuchengetera kana kuongororwa kunogona kukanganisa kugadzikana kwekuenzanisa, kunyanya pakudziya-tembiricha.

Zviratidzo: Kusvibiswa kwekuongorora kunotungamira kumhedzisiro isina kuvimbika.

Solution: Store samples pakurudziro yakakurudzirwa uye kuderedza mhedzisiro yekudziya kwekudziya panguva yekuongorora.

Kusarudza iyo kurudyi 2ML autosamppler vals

Kuti uderedze nyaya ne 2ML autosamupler vals, funga kuita zviitiko zvinotevera zvinotevera:

Kugara uchichengetera uye kuumbwa: Ronga nguva dzose kuchengetedza pane yako autosampler uye ita calibhurari zvichienderana nhungamiro yemugadziri.

Mamiriro Ekuchengetedza Akakodzera: Chitoro mavai munzvimbo yakachena, yakaoma nzvimbo kure nekureba kwezuva uye kupisa kwakanyanya.

Kusarudza iyo chaiyo vial mhando yekunyorera yako: Zvichienderana nekunyorera kwako (Hplc vs. gc)


Unoda kuziva mhinduro makumi mashanu nezve HPLC vials, ndapota tarisa chinyorwa ichi:50 Mibvunzo inowanzo bvunzwa paHPLC vials

Kugadzirisa nyaya dzakajairika ne2ml autosamppler valsinokoshesa kuchengetedza kurongeka uye kuvimbika mumhedzisiro yako ongororo. Nokunzwisisa zvinogona kuve nenyaya dzakadai sekuwedzera, kusasvibisa chisimbiso, kusvibiswa, zvibvumirano zvakakuvadzwa, uye mapundu asingatarisirwi, vashandisi vanogona kutora matanho ekugadzirisa kuti kuderedze matambudziko aya. Kuita zvakanakisa maitiro mukubata, kuchengetedza, uye kugadzirisa kuchawedzera kugadzirisa maitiro ako autosamppler uye kuve nechokwadi chekuyevedza zvemuviri. Kugara uchidzidziswa vashandi vekuramusha munzvimbo idzi kunogona zvakare kuderedza zvikanganiso zvakabatana neAutosamppler Vial yekushandisa.