Isampula vial inomthelela omkhulu. Kuthinta inqubo kanye nemiphumela ye-chromatography. Uma i-vial yesampula ihlanzwe ngokungalungile, izongcolisa. Lokhu kungcoliswa kungadala: iziqongo zesipoki, ukuwohloka kwesampula, ukulahleka kwesampula, ukuphindaphinda okungahambi kahle, okuphindaphindile kabi, futhi iziqongo ezibangelwa yi-solvent kanye ne-septum zisebenzisana. Ama-vials aphathwa ngokungafanele azothinta kakhulu imiphumela yokuhlola. Lokhu kuzodala ukuphambuka emiphumeleni futhi kulimaze ne-autosampler.

Ngakho-ke, ukuhlanzai-autosampler vialkubaluleke kakhulu. Umhloli kufanele akwazi kahle indlela yokuhlanza ye-vial.

Ufuna ukwazi ngokugcwele mayelana ne-HPLC VIALS, sicela uhlole le ndatshana: I-Encyclopedia of HPLC VIALS

Kanjani

Indlela yokuhlanza yehlukile ngokuya ngezinga lokungcoliswa kwe-vial. Lo mbhalo uzoncoma izindlela eziningi zokuhlanza i-vial. Bazokusiza ukuqeda isivivinyo se-chromatographic.

Indlela 1

1. Thela isixazululo sokuhlola ngaphakathiI-HPLC VIAL.

3. Thela emanzini ahlanzekile futhi uhlanze i-ultrasonically it kabili.

4. Thulula uketshezi lokuwasha bese ubhaka ku-110 degrees Celsius amahora angama-1-2 (ungabheki ekushiseni okuphezulu, okuzobangela ukulimala kwe-vial).

5. Okupholile futhi kugcina.

Indlela 2

1.Izikhathi eziningi ngamanzi ompompi.

2. Iyicwilise ku-beaker yamanzi anciphile futhi usebenzise i-ultrasonic ihlanza imizuzu eyishumi nanhlanu.

3. Cisha amanzi bese uyinika eminye imizuzu eyishumi nanhlanu yokuhlanzwa kwe-ultrasonic.

4. Faka i-vial e-anhydrol ethanol-egcwalisa ethanol.

5. Ekugcineni, yisuse futhi uyeke ukome ngomoya ngokwemvelo.

Indlela 3

2. Ngemuva kokungeza amanzi amaningi kwi-vial eyisampula, ihlanzele ama-ultrasonic imizuzu engama-20, bese ikhipha amanzi.

3. Vumelathe vialukoma.

Indlela 4

1. Hlambulula bese uyomisa ngamanzi ahlanzekile kuqala, bese uyifaka ku-ejenti yokuhlanza eqinile ye-oxidizing agent (potassium dichromate sulfate) isixazululo sokuhlanza.

Indlela 5

1. Shehlisa ku-ejenti yokuhlanza oxidizing eqinile amahora angama-24.

2. Hlanza amahlandla ama-3 ngamanzi e-deionized ngaphansi kwezimo ze-ultrasonic, bese ekugcineni uhlanzekile kanye nge-methanol, bese uyome ukuze uyisebenzise.

Indlela 6

Sebenzisa umshini wokugeza umshini. Umshini wokuwasha ibhodlela ungathuthukisa ukusebenza kahle kokuhlanza ama-vials bese ugcine amandla kanye nesikhathi.

Ngabe uyazi okuningi ukuthi uhlanze kanjani ama-HPLC VIALS akho? Bheka le ndatshana: Izindlela ezinhlanu zokuhlanza ze-HPLC VIALS

Izinkinga ongahlangabezana nazo

Kunezinkinga eziningi ngokuhlanza ngesandla.

1. Ukusebenza kahle okuhlangene, isikhathi eside sokugeza, isikhathi esidla isikhathi nomzamo. Ngaphezu kwalokho, inani lamabhulashi kanye nama-detegendents likhulu, kunzima ukuphatha, futhi libeka izinsiza zamanzi.

2. Ukuhlanza kuthambekele emakhoneni afile, umphumela wokuhlanza kunzima ukuqinisekisa, uthinta imiphumela yokuhlola, kanye nokwandisa amandla mabandla nezindleko ezibonakalayo.

3. Kunezingozi zokuphepha kwinqubo yokuhlanza yabasebenzi bokuhlanza abathile. Amanye ama-laboratories azosebenzisa imishini yokuhlanza ye-ultrasonic. Le ndlela yokuhlanza ithuthukisa ukusebenza kahle kokuhlanza nokuhlanzeka ngezinga elithile, kepha futhi inobunzima.

Umshini wokuhlanza we-ultrasonic unesisindo futhi unokhahlo ngesikhathi sokusebenza, futhi kulula ukuphula i-vial, nesikhathi sokuhlanza akulula ukuqonda. Ngakho-ke, sincoma ukuthi ugqoke amagilavu, ama-goggles, izindlebe kanye neminye imishini yokuvikela ukuphepha ngesikhathi sokuhlanza.

Uma i-vial indala noma yonakele, ungaphinde uyisebenzise. Kuya ngokuthi uvame kangakanani ukwenza ukuhlolwa, buyisela esikhundleniisampula vialnjalo ezinyangeni ezi-1-3.

Ama-vials alahliwe adinga ukuphathwa ngokulinganayo, aphathwe ngokuhambisana nemithetho ye-Laborary Enobungozi Yokulawulwa Kwemfucuza yemfucuza, futhi anikelwe ezinkampanini ezinobungozi zokwelapha imfucuza enobungozi yokulahlwa.

Indlela ngayinye yokuhlanza inezinzuzo ezihambisanayo nobunzima. Indlela engcono kakhulu ukufaka esikhundleni se-vial entsha ngemuva kokuhlolwa ngakunye. Kubalulekile ukuthi ukhethe inqubo yokuhlanza efanele. Ngokusekelwe kuhlobo lwesampula yokuhlola kanye nezimo zelebhu yangempela, lokhu kukhetho kufanele kwenziwe. Kuyalulekwa nokuthi ucabangele izindleko zecala. Kufanele kukhunjulwe ukuthi kulandela isivivinyo ngasinye se-chromatographic, i-septum ye-vial eyisampula idinga ukushintshwa.

Wan ukwazi ulwazi oluphelele lokuthi ungahlanza kanjani i-Chromatography Sampula ama-vials, sicela uhlole le ndatshana: Esebenzayo! Izindlela ezi-5 zokuhlanza i-chromatography isampula ama-vials

Okwedlule:

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