Musoro Sampling ndiyo nzira iyo inobvumira kuongororwa kweiyo kusiririsa mishonga mune yegesi chikamu pamusoro pemuenzaniso. Iyi nzira inonyanya kubatsira samples ine nonvocoles kana yakaoma matrices nekuti inobatsira kuderedza kuiswa kwekusvibisa muGC system. Nekuongorora chete chikamu chegasi chete, misoro yemuenzaniso inogona kupa jekiseni rakachena uye kuderedza zvinodiwa pakugadzirira kwemuenzaniso.
Unoda kuziva kuzere infor anoreva zvemusoro vial, ndapota tarisa ichi chinyorwa: Yakatemerwa Nhungamiro Kumusoro Musoro Viums: Zvimiro, Kusarudzwa, Mutengo, uye Kushandiswa
Static homkepace gc
MuStatic Musoro GC, sampuli yakaiswa mukatiVial yakavharwa, uye mishonga inosiririsa inobvumidzwa kuenzana pakati pemvura kana sosi yakasimba uye iyo gasi chikamu pamusoro payo. Vial inowanzo kupisa kusimudzira kusunungurwa, uye mushure mekutarisirwa kwenguva yakaenzana, chikamu cheMusoro gasi chinobviswa uye chakaiswa muGC system yekuongorora.
Kiyi yezvinhu zve static homnoce gc
Equilibrium-based: Static Pricepace inovimba neiyo nheyo yekuenzana, uko kuenderana kunoenderana neyekuparadzanisa kwemuenzaniso uye mumusoro. Izvi zvinoreva kuti kushushikana kwekuongorora mumusoro kuchaita kuti udzikise nekufamba kwenguva.
Sampule Kugadzirira: Kugadzirira Kwemamwe Sampuli kunodiwa, kuiita nzira yakatwasuka yekuongorora madhiri ehuremu mumatanho akaoma.
Vial kudziya: Vial inopisa kuti uwedzere kuderera kwemakomisheni, iyo inokwidziridza kusunungurwa kwavo mumusoro.
Zvishandiso: Static Pommentpace GC inowanzoshandiswa pakuongororwa kwemamwe mishonga yemishonga, flavor makomputa uye zvinwiwa, zvevakadzi) mune zvemamiriro ekunze.
Zvakanakira mitsipa yemusoro weGC
Kujekesa: Iyo nzira iri nyore kuita, inoda midziyo midiki uye matanho ekugadzirira.
Yakadzikira Kusvibiswa: Nekuongorora chete iyo iyo vapende chikamu, njodzi yekusvibiswa kubva kune isiri-yakajeka zvikamu zvinoderedzwa.
Kunzwa kwakanaka: Static Pommentpace inogona kupa kukwana kwakakwana kwemazhinji mishonga inosiririsa, kunyanya kana yakagadziriswa.
Kugumira kweiyo static homnoce gc
Nguva yekuenzana: Kuwana kuenzana kunogona kutora nguva, iyo inogona kunge isina kukodzera kune yakakwira-yekuchinjisa anoongorora.
YAKABVUNZWA KUTI VAVANZE Makomisheni: Static Pricepace inonyanya kushanda kune isina kujairika mishonga; zvisiri-zvisingaenzaniswi mishonga inogona kunge isina kunyatsomiririrwa mumusoro.
Unoda kuziva zvakawanda nezve nei mhirizi dzakashandiswa mu chromatography? Nei mishoms yemusoro inoshandiswa mu chromatography? 12 angles
Dynamic Musoro GC
Dynamic Musoro GC, kune rumwe rutivi, inosanganisira kuramba ichinge ichinyepedzera sampuro ine syter gasi, kazhinji nitrogen kana helium. Iyi gasi inotsvaira mishonga inosvibirira kubva mumuenzaniso mune yegomba chikamu, apo ivo vakazotumbuka uye vakanyudzwa vasati vabvumidzwa muGC system.
ZVINOKOSHA ZVINOKOSHA ZVEKUSVIRA Musoro UPRAMECE GC
Kuenderera mberi Kuchenesa: Mumusoro weDynamic, iyo Inerer Gasi inoenderera ichipfuura nemuenzaniso, kutakura mishonga inosiririsa muchikamu chegesi.
Trap Constrenration: Iyo isina kujairika mishonga inounganidzwa mumusungo, iyo inogona kupiswa gare gare kuti ideswe iyo fungidziro kune iyo GC Column yekuongorora.
Zvikumbiro: Musoro weDynamic zvinowanzoshandiswa kuongororwa kwekutarisa-mhepo inoshambidzika mumvura, mhepo, uye samples yakasimba, pamwe mukutsunga kwesimba-solubility compound.
Zvakanakira zveDynamic Musoro GC
Kunzwa kwepamusoro: Kuenderera mberi kuchenesa uye kuteedzera kwevanhurume kunogona kutungamira mukuvandudzwa kwekunzwa, zvichiita kuti ive yakakodzera kuongorora.
Kuongorora nekukurumidza: Musoro weDynamic kunogona kukurumidza kukurumidza kupfuura nzira dzemitambo, kunyanya kwemasampuli anoda kukurumidza kuongororwa.
Kuita
Kugumira kweDynamic Musoro GC
Kuomarara: Setup yeMusoro weDynamic inogona kuve yakaomarara, inoda zvimwe zvekuwedzera senge misungo uye gasi rinoyerera system.
Zvinogona Kurasikirwa: Kana zvisingakwanisi kudzorwa zvakanaka, kuchenesa kunoenderera kunogona kutungamira mukurasikirwa kwemakombi vashoma, kunyanya avo vane mapoinzi akaderera.
Kuenzanisa static uye dynamic hirdpace gc
| Chimiro |
Static homkepace gc |
Dynamic Musoro GC |
| Nheyo |
Equilibrium-based sampling |
Inoenderera ichitsvenesa ine inert gasi |
| Kuenzanisira Kugadzirira |
Kugadzirira kushoma kunodiwa |
Inoda kuseta kwegasi kuyerera uye kuteedzera |
| Kunzwa |
Zvakanaka kune vazhinji vashoma |
Kunzwa Kwakakwirira Kwekutsvaka-Level Kuongorora |
| Kuongorora Nguva |
Nguva yakareba yekuenzana |
Kazhinji nekukurumidza kuongorora |
| Zvishandiso |
Vakasara sol sol sol sol solvent, flavars, vocs |
Trace ongororo mumvura, mhepo, solids |
| Kuoma |
Simpler Setup |
Kuwedzeredza kuwirirana |
| Njodzi yekusvibiswa |
Yakadzika njodzi nekuda kwekuvharwa system |
Kugona kurasikirwa kweshoko |
Nguva yekushandisa static kana deynamic pamusoro gasi chromatography
Shandisa static mumusoro gasi chromatography kana:
Iwe unoongorora mishonga inosiririsa mumatanho akareruka.
Iwe unoda nzira yakapusa ine zvishoma kugadzirira kugadzirira.
Iyo mishonga yekufarira ndeye inoenderana zvakakwana kuti isvike kuenzana mukati menguva yakakodzera yenguva.
Iwe urikushandisa nzira yekudzora iyo inotsanangura static musoro kuongororwa.
Shandisa zvine simba mumusoro wegirazi chromatography kana:
Iwe unofanirwa kuongorora kuongorora kutevedza kusevha mune yakaoma matrices.
Iyo makomputa ekufarira ane yakaderera kuderera kana yakadzika mabhomba mativi uye inogona kunge isina kubatwa zvakakwana nemusoro wenyaya.
Kuongorora nekukurumidza kunodiwa uye iwe une iyo infrarture yekutsigira inoenderera mberi nekubatwa uye kubatwa.
Iwe urikushanda nemasangano akasimba kana matrices ayo anogona kuburitsa kusunungurwa nekufamba kwenguva.
Unoda kuziva nzira yekusarudza iyo yakakodzera cap yemusoro wako, ndapota tarisa ichi chinyorwa:Uri kusarudza iyo chaiyo cap yeMusoro wako Musoro Lial?
Mhedziso
Zvese zviri zviviri uye zvine simba mumusoro gasi chromatography maitiro anokosha ekuongorora zvisingaite makomputa, uye nzira imwe neimwe ine zvakanakira zvakasiyana uye zvisingakwanisi. Kunzwisisa misiyano pakati penzira mbiri kunobvumira vaongorori uye vanoongorora kuti vasarudze nzira yakakodzera kwazvo kune yavo chaiyo yekuongorora. Nekufunga nezvezvinhu zvakadai sekunzwa, kuomesa moyo, uye nguva yekuongorora, marebarendi anogona kuongorora masara avo uye anowana zvakaringana uye akavimbika mhedzisiro mukuongorora kwavo. Kunyangwe iwe uchisarudza static kana masheya eChromatography, nzira mbiri dzinoita basa rakakosha mumunda wekusvitsa kwekuongorora kwemakemikari, kupa nzwisiso muzvinyorwa uye mhando yemhando dzakasiyana siyana.
Chirungu
ChiChinese
