I-HPPC ye-VPLC

I-HPLC (i-chromatography ye-chromatography) i-vial fasts zezinto ezibalulekileyo kwi-chromatography, yenzelwe ukuphucula ukusebenza nokuchaneka kwesampula. Oku kufaka i-fakela ivumela inaliti echanekileyo yemithamo encinci yesampulu, nciphisa inkunkuma, kwaye uqiniseke ukuba ingqibelelo yesampulu igcinwa kuyo yonke inkqubo yohlalutyo. Eli nqaku likhangela iintlobo, izixhobo, izicelo, izibonelelo, kunye nezenzo ezilungileyo zeI-HPPC ye-VPLC.

Ufuna ukwazi ngakumbi malunga ne-HPLC vial vial vial, nceda ujonge eli nqaku:Ukufakwa kwe-HPLC: ukuphucula inyani kunye nempazamo yesampulu

Iifayile ze-HPLC ze-HPLC zizinto ezincinci ezibekwe ngaphakathiI-vials emiselweyo ye-HLLCUkufaka iisampulu kwinkqubo yeChromatography. Benza imisebenzi emininzi ephambili:

Ingxwabangqwa yesampula: Faka ukunciphisa ivolumu yegumbi lesampulu, kuvumela ukuba ugxile ngakumbi kuhlalutyi. Oku kuluncedo ngakumbi xa usebenza ngemiqulu encinci.

Nciphisa ilahleko yesampulu: ngokubonelela ngesithuba esincinci sesampulu, faka uncedo kunciphisa ukuphulukana nesampulu exabisekileyo ngexesha lenaliti.

Thintela ungcoliseko loMnqamlezo: Ukufakwa kunganceda ukukhusela ungcoliseko lwe-Cross phakathi kweesampulu ezahlukeneyo, ukuqinisekisa ukuthembeka kweziphumo zovavanyo.

Ukuhambelana neenkqubo zoxinzelelo oluphezulu: Ezi kufakwa zenzelwe ukumelana neengcinezelo eziqubisana nemisebenzi ye-HLLC kwaye zigcine ingqibelelo yazo phantsi kweemeko ezinzima.

Iindidi ze-HPLC

Zininzi iintlobo zeflc vial vial, nganye ilungiselelwe iimfuno ezithile zohlalutyo. Olona candelo lodidi lubandakanya:

I-1. Ukwahlulahlulwa kwezixhobo

Iglasi ifaka:

Uzinzo lweekhemikhali: Iglasi yokufakwa i-glass inomchasi ogqwesileyo kwaye unganxibelelani nezicoci ezininzi okanye uhlalutyi, uzinze zilungele izicelo ezicocekileyo.

Izicelo: Okusetyenziswa ngokuqhelekileyo kuvavanyo lwamachiza kunye nokutya okufuna ukuchaneka okuphezulu.

2. Ukwahlulahlula-hlulwa ngamacala asezantsi

I-Coyint Ezantsi:

Yenzelwe ukugxila iisampulu ezantsi, ukunciphisa iintsalela kunye nokwandisa ukubuyela kwimeko yesiqhelo. Ilungele ukuhlalutya ukulandelwa kwendawo nganye.

Ukufakwa kweflethi esezantsi:

Kulula ukucoca kwaye uphinde usebenzise, ​​kodwa ungashiya ulwelo olungaphezulu. Ilungele ukugcina ngokugcinwa ngokubanzi kunye nemisebenzi yokulungisa.

Isiseko somdibaniso kunye ne-Polymer Pentres:

Babonelela ngozinzo olongezelelekileyo lokuthintela ukutyibilika okanye intshukumo ngaphakathi kwe-vial, ibenza bafaneleke uhlalutyo lwegalelo eliphezulu.

I-3. Ukwahlulahlulwa ngobude

Ukufaka kwakhona kuza ubude okwahlukileyo ukulungiselela ubungakanani be-vial ye-Vial:

Ubude obuqhelekileyo bubandakanya i-5x29 mm kunye ne-6x29 mm, ehambelana neentlobo ngeentlobo ze-autosamplers kunye ne-vials.

Ukukhetha i-vial vial vial vial

Kukho izinto ezininzi ekufuneka ziqwalaselwe xa ukhetha i-HPPC ye-HPPL ye-HPPPC:

Ithamo yesampulu: kwimiqulu emincinci yesampulu, i-contral faw icetyiswa ukuba yandise kwakhona.

Ukukhuphela ikhemikhali: Iisampulu ezisebenzayo, ukufaka iiglasi kukhethwa, ngelixa izinyibilikisi ezingaphantsi, ukufaka iplastiki kunokusetyenziswa.

Iimfuneko zesicelo: Uhlalutyo oluchanekileyo lunokufuna ukuba ufike okanye ukwenziwa okukhethekileyo ukuphucula ukuchaneka kwemilinganiselo.

Ngaba ufuna ukwazi ukuba ndikhetha njani ilungelo lokufaka i-HPPC yam ye-HPPL? Nceda ujonge eli nqaku: Ndikhetha njani ilungelo lokufaka kwi-vial yam ye-HPPL?

Izibonelelo zokusebenzisa i-HPPC ye-HPPC

Ukufakwa kwe-vial factos kwi-chromatography yakho inika izibonelelo ezininzi:

1. Ukulondolozwa kwesampuli

Ngokunciphisa ivolumu efileyo ngaphakathi kwe-vial, faka uncedo lokugcina isampulu exabisekileyo, ebaluleke kakhulu xa usebenza ngamaxabiso abiza kakhulu okanye anqongopheleyo.

2. Ukuphuculwa ngokuchanekileyo

Faka ukunciphisa ukwahluka kwinaliti yesampulu ngokubonelela ngemivotisi yohlalutyo ngalunye, kukhokelela kwiziphumo ezinokuthenjwa, ezibuyisiweyo.

3. Ukuphucula imvakalelo

Iisampulu zokugxila kwimitha encinci iphucula imida yokuchonga imida yohlalutyo olusezantsi, ngaloo ndlela yandisa ubuntununtunu bendlela yakho yeChromatographic indlela yakho.

Ukusetyenziswa ngokuchanekileyo kunye nokugcinwa kwe-HPPC ye-HPPC

Ukwandisa intsebenzo kunye nobomi be-HPPC ye-vial, ukusetyenziswa ngokufanelekileyo nokulondolozwa kuyagxeka:

Ukucocwa rhoqo kubalulekile ukunqanda ungcoliseko: Ukufakwa kweglasi kunokucocwa ngeentsomi ezifanelekileyo ezingasasebenzi ngeglasi. Ukufakwa kweplastiki kuya kubanjwa ngokucokisekileyo ukususa nayiphi na intsalela eseleyo ukusuka kuhlalutyo lwangaphambili.

Ukuthintela ukuqaphela kwengzuzo: Soloko unxiba iigloves ezicocekileyo xa uphatha ukufaka. Kulumkele ukunxibelelana ngqo nomphezulu okanye umphezulu wangaphakathi we-vial.

Gcina indawo engasetyenziswanga kwindawo ecocekileyo, eyomileyo: Sebenzisa ukupakisha okukhuselekileyo ukuthintela umonakalo okanye ungcoliseko ngaphambi kokusetyenziswa.

I-HPPC ye-VPLC sisixhobo esibalulekileyo kwi-chromatography ephucula isampulu yokuphatha ngempumelelo kunye nokuchaneka kohlalutyo. Ngokuqonda iintlobo zabo, izixhobo, izicelo, kunye nezibonelelo, abaphandi banokwenza izigqibo ezinolwazi malunga nokusetyenziswa kwabo kwiindawo ezahlukeneyo zohlalutyo lweChromatographic. Ukukhetha okufanelekileyo kunye nokugcinwa kwezi kufakwa kunokuhamba indlela ende ekufumaneni iziphumo ezinokuthenjwa kwindawo yamayeza, okusingqongileyo, ukhuseleko lokutya, kunye nezicelo zophando. Njengokuqhubela phambili kwetekhnoloji, ukuqhubeka koyilo kuYilo lweLiqual Linerial kuya kuphucula ukusebenza kwabo ekuxhaseni umsebenzi osemgangathweni osemgangathweni osemgangathweni.

Ufuna ukwazi ukuba ukhethe indlela yokukhetha uhlobo olufanelekileyo lwe-Micro-fin ye-vials yakho ye-chromatography, nceda ujonge eli nqaku:Ungalukhetha njani uhlobo olufanelekileyo lwe-Micro-fin ye-vials yakho ye-chromatography yakho