Ungayenza njani ingxaki kwimiba eqhelekileyo ye-2ml automampler

I-autosampler vialszizinto ezibalulekileyo kwi-chemistry yohlalutyo, ngakumbi kwi-chromatography ye-chromatography (i-HPPC) kunye ne-chromatography yegesi (GC). I-2ml automampler vils yenye yezona ndawo zihlala zisetyenziswa kakhulu, kodwa imiba eyahlukeneyo inokuvela ngexesha lokusebenzisa kwabo. Esi sikhokelo sinika umbono obanzi wemicimbi eqhelekileyo enxulumene ne-2ml automampler vials kwaye ibonelela ngezisombululo ezigwenxa zokuqinisekisa ukusebenza kakuhle.

Ubume be-2ml automampler vials

Phambi kokuba ukuntywila kwingxaki, kubalulekile ukuqonda ulwakhiwo olusisiseko kunye nomsebenzi we-2ml autompler vials. Ezi vils zibandakanya:

Izixhobo: Uninzi lwenziwa ngeglasi ye-borossilicate, exhaphazi ngamachiza kwaye inciphise ukusebenzisana ngesampulu.

Uhlobo lweCAP: Ukukhetha kubandakanya i-CAPS ye-CAPS, i-CRIMP CAPS, kunye ne-Snap CAPS, inikela ngeendlela ezahlukeneyo zokutywina.

I-Septa: Icandelo elibalulekileyo elivumela ukungena kwinaliti ngelixa igcina itywina ukuthintela ukuthuma okanye ungcoliseko.

I-Wan Ukufumana ulwazi olupheleleyo malunga nendlela yokucoca i-vialsgraphy yesampulu ye-chromatography, nceda ujonge eli nqaku: Iyasebenza kakuhle! Iindlela ezi-5 zokucoca iimodeli ze-chromatographys

Iingxaki eziqhelekileyo kunye namanyathelo acociweyo

I-1. Ukunqanda i-vials

Ingxaki: Ukugqwetha okwenzeka xa inani lolwelo kwi-vial ligqitha amandla alo. Oku kubangela indawo yentloko engonelanga kwinaliti ye-autosampler yokusebenza ngokufanelekileyo.

Iimpawu: isampulu yesampulu engahambelaniyo, i-fereover ye-fereover, okanye inaliti ebekekileyo.

Isisombululo: Qiniseka ukuba i-vial izaliswe kwinqanaba elicetyiswayo, ngokuqhelekileyo malunga ne-1.5ml ye2ml ngel. Oku kubonelela ngeplate eyaneleyo yokufakelwa kwenaliti kunye nokufuduka kwesampula.

I-2. Ungcoliseko lwesampulu

Ingxaki: Ungcoliseko lunokwenzeka ekuphathweni okungafanelekanga, i-vials ephantsi, okanye ukutywina ngokwaneleyo.

Iimpawu: Iincopho ezingalindelekanga kwindawo yeChromatogram okanye yesampulu eguqulweyo.

Isisombululo: SebenzisaI-Vials esemgangathweni ephezulu kunye ne-capsyenzelwe isicelo sakho. Soloko uphatha i-vials ngeegloves kwaye uphephe ukuchukumisa iindawo zangaphakathi. Cinga ngokusebenzisa i-vials ecocekileyo okanye eqinisekisiweyo ukunciphisa umngcipheko wongcoliseko.

3. Iincopho ezingalindelekanga kwiiChromatograms

Ingxaki: Iincopho ezingalindelekanga zinokubonisa ungcoliseko okanye i-cartover ukusuka kwiisampulu zangaphambili.

IZIXHOBO ZOKUGQIBELA:

Amacandelo acocekileyo acocekileyo rhoqo: Ukuphunyezwa kweshedyuli yokucoca yonke imihla yezinto ze-andesampler, kubandakanya isirinji kunye neenaliti.

Sebenzisa i-vials ye-vials ye-vials ephantsi: Khetha i-vials yokubuyisela ePhakamileyo eyenzelwe ukunciphisa ivolumu yendawo kwaye ke inciphise umngcipheko we-rossover.

I-4. I-Benle Block

Ingxaki

Iimpawu: Akukho sampula ifakwe okanye ivolumu yenaliti yimpazamo.

Isisombululo: Isihluzi sesampulu sisebenzisa iphepha lesifiso okanye i-membrane yokususa iinkcukacha ngaphambi kokuyibeka kwi-vial. Ukuba ubukhulu beka, coca inaliti ngokwemiyalelo yomenzi kwaye uqwalasele usebenzisa inaliti enkulu ye-bore ye-Vicous.

I-5. Ukuqhekeka koqhawulo-mtshato

Ingxaki:Iglasi ngelsinokuqhekeka ukuba iphantsi koxinzelelo olugqithisileyo, ukothuka, okanye ukuphatha kakubi.

Iimpawu: Umonakalo obonakalayo ngokuhlola; Isampulu inokulahleka.

Isisombululo: Chukumisa i-vial ngononophelo kwaye uphephe utshintsho lobushushu ngequbuliso. Sebenzisa isiciko esikhuselayo ukuba kukho imfuneko ngexesha lothutho okanye lokugcina.

I-6. Ukunyaniseka okungalunganga

Ingxaki: Amatywina angonelanga anokukhokelela ekugxothweni kwezinto eziguqukayo okanye ungcoliseko oluvela kwimithombo yangaphandle.

Iimpawu: Iinguqu kuhlalutyo ekuhlalutyo ekuhambeni kwexesha; Ukuphulukana nobume beengcongconi.

Isisombululo: Qinisekisa ukuba i-CAPS iyahambelana nohlobo lwe-Vial kwaye iqinile ngokufanelekileyo. Ukuba uphatha iisampulu eziguqukayo, cinga ngohlobo lweCAPS yeTrimpp ukuze usebenzise ingqibelelo.

Ufuna ukwazi ukuba ukhethe njani i-cap ye-cap ye-chromatography yakho, nceda ujonge eli nqaku: Ungayikhetha njani i-cap cap ye-vials yakho yeChromatography?

7. Ukungahambelani ne-autosamplers

Ingxaki: Ayizizo zonke ii-vials ezihambelana nayo yonke imodeli ye-autsampler, enokubangela imiba yoomatshini ngexesha lokusebenza.

Iimpawu: Ukungasebenzi kakuhle kwee-vials okanye ukungakwazi ukufaka iisampulu.

Isisombululo: Qinisekisa ukuhambelana kohlobo lwe-Vial nemodeli ye-autosampler ngaphambi kokusetyenziswa. Jonga kwiSikhokelo soMvelisi kwi-vials encomekayo.

8. Ukuxinana kobushushu

Ingxaki: Inguqulelo yobushushu ngexesha lokugcina okanye uhlalutyo lunokuchaphazela uzinzo lwesampulu, ngakumbi ukudityaniswa kobushushu obuthathaka.

Iimpawu: Ukonakaliswa kohlalutyi okhokelela kwiziphumo ezingenakuthembeka.

Isisombululo: Gcina iisampulu kwiqondo lobushushu elicetyiswayo kwaye unciphise iziphumo zokuguquguquka kobushushu ngexesha lohlalutyo.

Ukukhetha i-vials ye-automampler

Ukunciphisa imiba nge-2ml automampler vials, cinga ngokuphunyezwa kwezi zinto zilandelayo:

Ukulungiswa rhoqo kunye nokulinganisa: cwangcisa ulondolozo rhoqo kwi-autosampler yakho kwaye wenze i-calibus ngokwesikhokelo somenzi.

Iimeko ezifanelekileyo zokugcina: I-Vials yeVenkile kwindawo ecocekileyo neyo eyomileyo kude nelanga ngokuthe ngqo kunye nobushushu obukhulu.

Ukukhetha uhlobo lwe-Vial Logiker of Spreen


Ufuna ukwazi iimpendulo ezingama-50 malunga nee-vials vials, nceda ujonge eli nqaku:I-50 kakhulu imibuzo ebuzwa rhoqo kwi-vials ye-HPPL

Ukujongana nemicimbi eqhelekileyo ngeI-2ml automampler vialsKubalulekile ukugcina ukuchaneka kunye nokuthembeka kwiziphumo zakho zohlalutyo. Ngokuqonda imiba enokubakho enjengokutyhileka, ukungcola, ungcoliseko, iinambu ezionakalisiweyo, ii-inales ezonakalisiweyo, kunye neencopho ezingalindelekanga, abasebenzisi banokuthatha amanyathelo asebenzayo ukunciphisa le miceli mngeni. Ukuphunyezwa kweendlela ezilungileyo zokuphatha, ukugcinwa, kunye nokulungiswa kuya kuphucula ngakumbi ukusebenza kwenkqubo yakho ye-automanter kwaye kuqinisekiswe iziphumo ezisemgangathweni. Uqeqesho oluqhelekileyo lwabasebenzi belebhu kwezi ndawo lunokukunciphisa kakhulu iimpazamo ezinxulumene nokusetyenziswa kwe-autosampler vial.